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Fig. 5. Bis(1-formylisoquinoline thiosemicarbazone)nickel(II), [Ni(21-H)2 ] Structural and Physical Correlations 41 The electronic spectra and magnetic susceptibility of [Ni(21)CIE] were found to be consistent with a five-coordinate high spin complex. This complex has greater antitumor activity against P388 lymphocytic leukemia test system in mice than cobalt(II), copper(II), zinc(II) and platinum(II) complexes of 21 [187]. Although 4-methyl-5-amino-l-formylisoquinoline thiosemicarbazone, 22, also forms [Ni(22)CIE] with chemical properties similar to [Ni(21)Clz], it, along with other metal complexes of 22, showed no activity against P388 lymphocytic leukemia test system in mice [202].

However, these transitions involve either the conformational change between paramagnetic tetrahedral and diamagnetic planar isomers in four-coordinate d 8 complexes [1, 2] or the change between paramagnetic five- or six-coordinate complexes and diamagnetic planar fourcoordinate d s species [3]. A small number of examples has been reported even for 4d element complexes such as those of molybdenum(II) [4] and for clusters such as Nb6Ill and HNb6Ill [5]. Most complexes showing spin-state transitions are in fact of low symmetry.

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Complex Chemistry

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